HT3 Headspace Probengeber

The HT3 incorporates traditional static headspace with the option to perform dynamic headspace.

In the static set up, a sample is placed in a vial and then delivered to the autosampler. Once in the autosampler, the vial is loaded into a platen for heating. Upon reaching the final heat time it is then mixed for a set period of time. Using an electronic Mass Flow Controller the static vial pressure is recorded and the sample is pressurized to a user-defined set point. Next, the sample is passed through a fixed volume loop to another user-defined final pressure set point. The loop containing the sample is then placed in line with the GC column for separation and detection.

In the Dynamic mode, upon completion of heating and mixing, the headspace is continuously swept with an inert sample gas that is routed through a sorbent trap thus removing more of the analyte and concentrating it on the trap. The trap is then heated and back-flushed to the GC column for separation and detection.

Static Headspace analysis is a time-tested and robust technique for the analysis of volatile compounds in almost any matrix. The popularity of the technique is due to Headspace analysis providing a clean, reliable result.

Teledyne Tekmar draws on our experience as a leader in low-level VOC analysis with the introduction of a next generation Headspace instrument, the HT3™ Static and Dynamic Headspace System.

Dramatic improvements in sensitivity are achieved with the new Dynamic Headspace option, while maintaining the ruggedness and reliability of a traditional Static Headspace instrument.

Autosampler Capacity	60-positions
Platen Heater	Up to 10 vials simultaneously heated up to 300° C via resistance heater settable in 1° C increments with a +/- 0.1° C uniformity
Vial Size	9, 12, 22mL vials accepted (9mL and 12mL vials require inserts)
Sample Loop	Ships with a 1mL Siltek® coated loop. Other optional loop sizes include 100, 250, 300, and 500μL as well as 2, 3, and 5mL
Sample Mixing	Optimix system allows variable power settings from 1 to 10
Display	Electronic status panel on the front of the unit
Trap Furnace	Controlled temperature range up to 300° C (Trapping Module only)
Trap Size	12 in (30.5 cm) x 1/8 in (0.32 cm) O.D.
Sample Pathway	Siltek® Tubing. Entire sample pathway temperature controlled up to 300° C
Software	21 CFR Tools Available
GC Interface	Interface to virtually all commercially available GC instruments. Supplies or accepts GC and Data System start/ready signals via software selectable GC I/O configuration
Valving	24 VDC motor actuated 8-port valve with removable rotor. Temperature controlled from ambient to 300° C
Data Input	Input via RS 232 or Ethernet TCP/IP using a PC with the HT3 Headspace TekLinkTM software running on Microsoft Windows XP Pro or greater
VOC TekLink™ Control of Gas Flow and Pressure	Gas flow controlled via Electronic Mass Flow Controller capable of flow rates from 5 to 500mL/min. +/- 2% of full scale
Voltage Requirements	100/115 VAC +/- 5%, 50/60 Hz 10 amps 220/240 VAC +/- 5%, 50/60 Hz, 5 amps
Gas Requirements	99.999% Helium or Nitrogen at 65-100 psi
Unit Dimensions	21 5/8 in (54.9 cm) H x 19 in (48.3 cm) W x 25 in (63.5 cm) D
Weight	86 lbs. (39 kg)
Environmental Conditions	This system is capable of operating in laboratory temperatures between 10° and 30° C and a humidity range from 10 and 90%
Corrosion Resistance	Front cover is resistant to aqueous samples with pH range of 1-10

Teflon® is a registered trademark of Dupont, Windows® is a registered trademark of Microsoft, PEEK™ is a trademark of Victrex PLC, Carbopack™ is a registered trademark of
Sigma-Aldrich®. Siltek® is a registered trademark of Restek. TekLink™ is a registered trademark of Teledyne Tekmar Company. Covered by one or more of the following patents:
7,651,866 and other patent pending.

Folgende Anwendungsdatenblätter sind für den HT3 bei ANTEC GmbH erhältlich.
Bitte fordern Sie diese bei Interesse per E-Mail bei uns an.

Application Notes HT3

Meeting the Korean Method ES 04605.3 for Formaldehyde (폼알데하이드) with Static Headspace GC/MS
Determination of Hexanal in Foods Utilizing Dynamic Headspace GC/MS
Meeting the Korean Method EX 04607.1 for Naphthalene with Static and Dynamic Headspace GC/MS
Meeting the Korean Method ES 04602.1b for Vinyl Chloride, Acrylonitrile, and Bromoform with Static and Dynamic Headspace GC/MS
Meeting the Korean Method ES 04601.2 for 1,4-Dioxane with Static and Dynamic Headspace GC/MS
Meeting the Korean Method 04603.2b for 12 VOC with Static and Dynamic Headspace GC/MS
Alcoholic Beverage Fusel Alcohol Testing with Static Headspace

Achieving Low-Level Detection of Benzene in Beverages with an Automated Headspace Vial Sampler
Methanol in Biodiesel by EN14110 with the HT3 and Versa Automated Headspace Analyzers
Blood Alcohol Determination with The Teledyne Tekmar HT3 and Young Lin YL6500 Gas Chromatograph
Residual Solvents Testing ASTM F1884-04 with the Versa and HT3 Automated Headspace Sample
Alternative Methods to RSK 175 Using Purge and Trap Concentration and Automated Headspace for the Analysis of Dissolved Gases in Drinking Water
Alternative Methods to RSK 175 Using Purge and Trap Concentration and Automated Headspace for the Analysis of Dissolved Gases in Drinking Water
Comparing US EPA and FDA Methods for 1,4-Dioxane in Consumer Product
Two Headspace Solutions for the Analysis of Dissolved Gases in Water by Method RSKSOP-175
Comparison of Static and Dynamic Headspace for Volatile Organic Compounds in Orange Juice
Comparison of BTEXS in Olive Oils by Static and Dynamic HT3 Headspace
Evaluation of a New Analytical Trap for Gasoline Range Organics Analysis
Bath Salt Characterization using the Tekmar HT3 Headspace Analyzer GC/MS
Using the Teledyne Tekmar HT3 Headspace Analyzer to Meet the Requirements of the Korean Standard Method for Water Pollution, ES04602.1 for Bromoform, Vinyl Chloride and Acrylonitrile
Using the Teledyne Tekmar HT3 Headspace Analyzer to Meet the Requirements of the Korean Standard Method for Drinking Water, ES05602.3 for 1,4-Dioxane
Evaluating Food Products for Furan and Other Volatile Organic Compounds
Evaluating Consumer Products for Low Level Contaminants with High Temperature Dynamic Headspace
A Survey of Residual Solvents in Various Inks used in Consumer Product Packaging
USP <467> Headspace Residual Solvent Assay
High Temperature Headspace Assay of Polymers
Headspace Assay of Polymers used in the Automotive Industry
Headspace Assay of Household Interior Paint
Determination of Furan in Coffee by Static and Dynamic Headspace GC-MS
Gasoline Range Organics (GRO) by Headspace/GC/FID
Detection Limits of EPA Method 8260 with Static and Dynamic Headspace GC/MS Analysis
Blood Alcohol Determination with Teledyne Tekmar HT3 Automated Static/Dynamic Headspace Analyzer
Determining Volatile Organic Compounds from Difficult Soil Matrices Utilizing both Headspace and Purge and Trap Techniques
Headspace Analysis of Volatile Organic Compounds (VOCs) in Contact Packaging Materials Using the HT3 Automated Headspace Analyzer
A Comparative Analysis of Fuel Oxygenates in Soil by Dynamic and Static Headspace Utilizing the HT3 Automatic Headspace Analyzer
Detection Limits of EPA Method 8260 with Static and Dynamic Headspace GC-MS Analysis

Autosampler - The HT3 comes with a standard integrated, 60-position autosampler, providing true walk away automation. Vials are automatically queued into the platen heater ensuring reproducible dwell times. Vials may also be added during a run to increase productivity. (Optional 9 or 12mL vial inserts sold separately.)

Valve/Loop System - The HT3’s valve and loop sample method has proven to be the industry’s most reliable technique for headspace sampling. The entire sample path is Siltek™ and can be heated up to 300oC thus minimizing analyte carryover. Different loop sizes ranging from 100μL to 5mL may be used depending on application.

Removable Sample Path - Easy access to sample path allows for trouble-free removal, maintenance and safety.

Platen Heater - The platen heater offers a 10-position, highly regulated heating chamber. Temperatures are controlled up to 300oC in increments of 1oC. A strict control of the platen heater chamber allows for superior reproducibility in sample preparation achieving greater sample accuracy.

Electronic Mass Flow Controller (MFC) - The patented MFC has the ability to control pressure and flow to assure consistent volume control regardless of external conditions for all samples.

Two-Stage Needle - This unique design allows for the continuous sweeping so critical to dynamic headspace analysis.

Trap - Sorbent traps allow for dynamic compound concentration and are available in a variety of sorbent packing materials. Some typical sorbents are listed below:
• Tenax - General purpose trapping agent
• Silica Gel - Choice for polar compounds
• Carbopacks™ - Variety of types for extended range compound trapping capabilities
• Carbo Sieve III - Extremely strong sorbent for extremely volatile compounds

Dynamic Option – This dynamic headspace sampling option concentrates the headspace sample and thereby increases your sensitivity requirements compared to that of the conventional static mode. Dynamic headspace allows for flexibility by allowing the user to set up a schedule utilizing both static and dynamic modes interchangeably.

Variable Fill Pressure Control – (patent pending) Utilization of a Mass Flow Controller, which reads and controls both pressure and flow in order to meet user-defined requirements for pressurization loop filling and static pressure assuring sample volumes are consistent from one sample injection to another.

ANTEC GmbH Analysen- und Prozesstechnik

Der HT3 vereint traditionelle statische mit dynamischer Headspace-Probenvorbereitung mit einem Probengeber mit 60 Positionen. Temperaturen von bis zu 300°C können im gesamten Probenweg konstant gehalten werden.

HT3 Static and Dynamic Headspace Vial Sampler

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